Download e-book for kindle: How an Economy Grows and Why It Doesn't by Irwin A. Schiff, Vic Lockman

By Irwin A. Schiff, Vic Lockman

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D . Chemistry i n Canada, (19767, 28, 19. Lemieux, R . U . , K u l l i n g , R . K . , Bernstein, H . J . , and Schneider, W . G . , J . Am. Chem. S o c . , (1958), 80, 6089. Karplus, M . , J. Chem. , (1959), 30, 11. Karplus, M . Am. Chem. S o c . , (1963), 85, 2870. H a l l , L . D . , Steiner, P . R . , and Pedersen, C . , Can. J . , (1970), 48, 1155. F a r r a r , T . C . , and Becker, E . D . , "Pulse and Fourier Transform N . M . R . " , Academic Press, New York, N . Y . , 1971. Cooley, J .

The r e a c t i o n o f 1, 6 , 6 ' - t r i - O - t r i t y T s u c r o s e w i t h 2 , 2 - d i m e t h oxypropane—N,N-dimethylformamide—j>-toluene s u l f o n i c a c i d a t room t e m p e r a t u r e , a f t e r a c e t y l a t i o n and c h r o m a t o g r a p h y on s i l i c a g e l , gave 2 , 3 - 0 - i s o p r o p y l i d e n e - l , 6 , 6 ' - t r i - O - t r i t y l s u c r o s e t r i - a c e t a t e and 3 , 4 - 0 - i s o p r o pylidene-T' ,6 , 6 ' - t r i t y l s u c r o s e t r i - a c e t a t e i n y i e l d s of 24% a n d 2 0 % , r e s p e c t i v e l y ( 3 5 ) .

The p r o t o n Rev a l u e s f o r (A) w e r e d e t e r m i n e d a t 3 6 0 MHz a n d t h e d a t a a r e g i v e n beTow ( i n m s e c ~ l ) . I t w i l l be r e c a l l e d t h a t these composite R^-values s h o u l d be dominated by neare s t - p r o t o n i n t e r a c t i o n s and, hence, those protons w h i c h a r e c l o s e s t t o g e t h e r s h o u l d r e l a x t h e most r a p i d l y , t h a t i s have t h e h i g h e r R^-value. I n accord with t h i s e x p e c t a t i o n , t h e H-6p p r o t o n s o f t h e g a l a c t o p y r a n o s e r i n g o f (A) r e l a x m o r e r a p i d l y t h a n t h e o t h e r r i n g protons o f that moiety.

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