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M . Burlitch, /. Am. Chem. Soc, 89, 4953 (1967). 11 W. H . Atwell, D . R. Weyenberg and J . G. U h l m a n n , / . Am. Chem. Soc. 91, 2025 (1969). 12 W . H . Atwell and J. G. U h l m a n n , unpublished studies. 13 M . E. Volpin, Yu. D . Koreshkov, V . G. Dulova and D . M . Kursanov, Tetrahedron, 18, 107 (1962). 14 E. G. Janzen, J. B. Pickett and W. H . Atwell, / . Am. Chem. Soc, 90, 2719 (1968). 15 P. S. Skell and E. J . Goldstein, / . Am. Chem. Soc, 86, 1442 (1964). 16 O . M . Nefedov and M .

317 κ. Si' / ^Me R Me P\rí \ Me Ph SiC^ Ph ANDRIANOV Me Ph \ Α. p. 0. p. 74<' U n d e r these conditions isomer I converted into the polymer with T^sp = 0-24 {Figure 5, curve I) and the molecular weight of 164000. After 30 minutes polymerization isomer I I had T^sp. = 0-21 {Figure 5, curve 2). Table 5. Cyclotetrasiloxane polymerization in the presence of catalyst HO(CH3C6H5SiO)8K No. Polymerization time, min. Monomer Tetramethyltetraphenylcyclotetrasiloxane* 2,4,6',8'-tetramethyl-2',4',6,8-tetraphenylcyclotetrasiloxane 2,4,6,8-tetramethyl-2',4',6',8'-tetraphenylcyclotetrasiloxane 2',4,6',8-tetramethyl-2,4',6,8'-tetraphenylcyclotetrasiloxane Mol.

So I hope I a m not mistaken if I interpret the term "organosilicon" in the classical meaning: chemistry of non silicatic compounds, of volatile, covalent silicon compounds comparable to the volatile compounds of carbon. Accordingly I should like to tell you at the end of my lecture something about lithium bis (trichlorosilyl) amide, a sole inorganic SiN compound. It can easily—and in high yield—be prepared by the reaction of hexachlorodisilazane with butyllithium, a n d no Gl substitution on the silicon takes place during this reaction.

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